Xylene/80 Charge all materials to a 2-liter reactor fitted with thermometer, stirrer, and inert gas inlets. Adjust inert gas to 0.15 l/min. Heat to 240'C (464'F) and hold until an acid number of 4-8 is reached. Cool and reduce to 70% solids with mineral spirits (KB-38). Approximate time of reaction is 7-9 hr. FORMULA No.4 (Flat Wall Phthalic Anhydride/435 "Acintol" Tall Oil Fatty Acid/812 Phthalic Anhydride/370 Pentaerythritol, Technical/288 Glycerol, 99%/276 "Acintol" D29LR/660 "Acintol"/336 Phthalic Anhydride/444 Pentaerythritol Technical/246 Ethylene Glycol/93 "Acintol"/714 Phthalic (anhydride)/444 Pentaerythritol (technical)/282 Xylene/80 Ethylene Glycol/75
配制方法:
Fusion Cook: Charge all ingredients to a four neck 2-1 reactor fitted with stirrer, thermometer, inert gas inlets and 18'' air condenser. Adjust gas flow at 0.1 liters/min. Heat to 210'C (410'F) and hold for 1 hr. Then heat to 240'C (464'F) and hold for acid number of 10-15. Cool and reduce with odorless mineral spirits to 30% "Amsco" 140.