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配方类型:
ELASTOMERS, PLASTICS, AND RESINS
配方说明:
Vinyl-Acrylic Copolymer for Contact Adhesive (Soft, flexible
inyl-acrylic with high tack)
配方组成:
Methacrylic Acid/2.400
"Abex" VA-50/38.00
2-Ethylhexyl Acrylate/348.00
N-Methylol Acrylamide (60% sol'n.)/2.00
Na2S2O8/1.25
Vinyl Acetate/149.00
Water/410.00
Form A solution of "Abex" VA-50 and N-methylol acrylamide in 150 g
of water. Blend monomers and form pre-emulsion by slowly adding the
mixture to the surfactant solution while agitating vigorously. Add
preemulsion to an addition funnel. To a 1 l resin kettle reactor add 220
g of water and Na2S2O8. Heat to 60'C while stirring and purging with
nitrogen. Prepare a solution of NaHSO3 in 40 g of water and charge to an
addition funnel. When the reaction temperature has reached 60'C charge
5.0 ml of the NaHSO3 solution and then begin addition of pre-emulsion.
Schedule addition time for about 3 h. Maintain polymerization
temperature at 65-70'C. The remaining NaHSO3 solution is added in 5.0 ml
increments throughout the reaction as needed. After all ingredients have
been add
配制方法:
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