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配方类型:
ELASTOMERS AND PLASTICS
配方说明:
Vinyl Acetate-Sodium Vinyl Sulfonate Copolymer
配方组成:
D: Sodium Vinyl Sulfonate (25.0% aq. sol'n.)/5.0
B: "Abex" 18-S (35% active)/8.2
E: Potassium Persulfate/0.6
F: Sodium Bisulfite (2% sol'n.)/0.5
C: Vinyl Acetate/95.0
A: Water/q.s.to 38%
配制方法:
Purge water (A) for 20 min with nitrogen. Add the "Abex" surfactant (B) and 25% of the vinyl acetate/SVS mixture (C, D). Purge for another 5 min with nitrogen. Heat the reaction mixture to 55'C and add the potassium persulfate initiator (E). Allow the potassium persulfate catalyst to mix for a few minutes and then add 10% of the sodium bisulfite activator solution (F). When the temperature increases a few degrees, begin the addition of the monomer mixture (C, D) and activator (F) concurrently. Control between 68-72'C for the remainder of the addition period (about 1 h). Heat the latex to 80'C for 1 h. Cool to room temperature and filter.
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