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4-sec-butyl aniline (B) (1.49 g, 10.0 mmol) was added to a solution of isatoic anhydride (A) (1.63 g, 10.0 mmol) in anhydrous DMF (40 mL) and the reaction mixture was stirred at 115° C. for 16 hours under nitrogen. It was then cooled to room temperature and poured into water (200 mL), and extracted with ethyl acetate (200 mL). The organic phase was washed with water (100 mL), 10% aqueous NaOH solution (100 mL), water (100 mL) and dried over anhydrous Na2SO4. Removal of solvent gave 2-amino-N-(4-
| 产品 | |
| 反应物 |
4-sec-butylaniline isatoic anhydride water |
| 试剂 |
dimethylformamide |
| 程序 |
1、Add 4-sec-butyl aniline (B) (1.49 g, 10.0 mmol) was added to a solution of isatoic anhydride (A) (1.63 g, 10.0 mmol) in anhydrous DMF (40 mL) 2、Stir the reaction mixture was stirred at 115° C. for 16 hours under nitrogen 3、Cool It was then cooled to room temperature 4、Add poured into water (200 mL) 5、Extract extracted with ethyl acetate (200 mL) 6、Wash The organic phase was washed with water (100 mL), 10% aqueous NaOH solution (100 mL), water (100 mL) 7、Dry dried over anhydrous Na2SO4 8、Remove Removal of solvent 9、Yield gave 2-amino-N-(4-sec-butylphenyl)benzamide (C) as a brown solid |
角色：product
分类：产品
实体类型：definiteReference
角色：reactant
分类：原料
实体类型：definiteReference
角色：reactant
分类：原料
实体类型：definiteReference
角色：reactant
分类：原料
实体类型：exact
角色：solvent
分类：催化剂
实体类型：exact