Ethylene glycol/41.120 React dimethyl terephthalate, ethylene glycol and zinc acetate with agitation for 5 hours to a maximum temperature of 210'C during which time the theoretical amount of methanol (836 ml) distills over. Add "M&T" color Suppressant-190 to deactivate the first stage catalyst. 2nd Stage Polyethylene terephthalate is prepared by reacting the following materials Dimethyl terephthalate/58.830 Ethylene glycol/41.120 Zinc acetate (catalyst)/0.009 "M&T" Color Suppressant-190/0.040 Zinc acetate (catalyst)/0.009 Dimethyl terephthalate/58.830 Bis 2-hydroxyethyl terephthalate/99.700 Titanium dioxide (delusterant)/0.250 "M&T" Catalyst S-21/0.102 Bis 2-hydroxyethyl terephthalate/99.700 Titanium dioxide (delusterant)/0.250 "M&T" Catalyst S-22/0.343 "M&T" RS-190 (color suppressant)/0.040
配制方法:
React the above materials with agitation in a stainless steel reactor at 280'C and 0.5 millimeters vacuum until the desired intrinsic viscosity is obtained.